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HRID1351838

反应详情

EQUATION

反应方程式

HRID 1351838 的结构方程式

REACTANTS

反应物

2
结构：[NH4+].[OH-]
HCID14923

Ammonium hydroxide

H5NO

结构：CCOC(=O)COc1ccc2c(c1)CC(NCc1ccccc1)CCC2
HCID18007287

未命名化合物

PRODUCTS

生成物

1
结构：NC(=O)COc1ccc2c(c1)CC(NCc1ccccc1)CCC2
HCID18007209

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

A solution of 2-(8-benzylamino-6,7,8,9-tetrahydro-5H-benzocyclohepten-2-yloxy)acetic acid ethyl ester (320 mg) and 28% ammonium hydroxide (1 ml) in methanol (3 ml) was stirred at room temperature for 12 hours. The mixture was evaporated in vacuo to give 2-(8-benzylamino-6,7,8,9-tetrahydro-5H-benzocyclohepten-2-yloxy)acetamide (270 mg).

WORKUP

后处理

  1. customThe mixture was evaporated in vacuo