4-Aminopyridine → HCID 17838231, compound

HRID 1352116Notes

Reaction equation

HRID 1352116 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][N:5]=[CH:4][CH:3]=1.[CH:8]([C:11]1[CH:16]=[CH:15][CH:14]=[C:13]([CH:17]([CH3:19])[CH3:18])[C:12]=1[N:20]=[C:21]=[O:22])([CH3:10])[CH3:9]>C1(C)C=CC=CC=1>[CH:8]([C:11]1[CH:16]=[CH:15][CH:14]=[C:13]([CH:17]([CH3:18])[CH3:19])[C:12]=1[NH:20][C:21]([NH:1][C:2]1[CH:7]=[CH:6][N:5]=[CH:4][CH:3]=1)=[O:22])([CH3:9])[CH3:10]

Participants

4

Reactant 2

HCID 17274-AminopyridineHCID 922592,6-Diisopropylphenyl isocyanate

Product 1

HCID 17838231HCID 17838231, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Conditions

Temperature
110 °C

Procedure

4-Aminopyridine (100 mg, 1.06 mmol) and 2,6-diisopropylphenyl isocyanate (216.0 mg, 1.06 mmol) were dissolved in toluene, and the mixture was then stirred at 110° C. for 4 hr.

Sources & evidence

ORD record
ord-ca0fb50b553f42d9a804cbe8b7a3e34d
Source dataset
uspto-grants-2007_05
Patent number
US07217722B2

Reaction notes

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