4-Aminopyridine → HCID 694486, compound

HRID 1352117Notes

Reaction equation

HRID 1352117 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][N:5]=[CH:4][CH:3]=1.[CH3:8][O:9][C:10]1[CH:15]=[CH:14][C:13]([N:16]=[C:17]=[O:18])=[CH:12][CH:11]=1>C1(C)C=CC=CC=1>[CH3:8][O:9][C:10]1[CH:15]=[CH:14][C:13]([NH:16][C:17]([NH:1][C:2]2[CH:7]=[CH:6][N:5]=[CH:4][CH:3]=2)=[O:18])=[CH:12][CH:11]=1

Participants

4

Reactant 2

HCID 17274-AminopyridineHCID 794431-Isocyanato-4-methoxybenzene

Product 1

HCID 694486HCID 694486, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Conditions

Temperature
110 °C

Procedure

4-Aminopyridine (100 mg, 1.06 mmol) and 4-methoxyphenyl isocyanate (158.5 mg, 1.06 mmol) were dissolved in toluene, and the mixture was then stirred at 110° C. for 4 hr.

Sources & evidence

ORD record
ord-e16c900c03b949d5b8c925105957dcb0
Source dataset
uspto-grants-2007_05
Patent number
US07217722B2

Reaction notes

Loading…