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HRID1352251

反应详情

EQUATION

反应方程式

HRID 1352251 的结构方程式

REACTANTS

反应物

2
结构：CCC(C)O
HCID6568

2-Butanol

C4H10O

结构：CS(=O)(=O)c1ccc(Cl)c(C(=O)O)c1
HCID2329132

2-chloro-5-(methylsulfonyl)benzoic acid

C8H7ClO4S

PRODUCTS

生成物

1
结构：CCC(C)Oc1ccc(S(C)(=O)=O)cc1C(=O)O
HCID21100258

未命名化合物

PROCEDURE

实验过程

Prepared in analogy to Example A1 (b) from 2-chloro-5-methanesulfonyl-benzoic acid (Example A1(a)) and rac-butan-2-ol. The crude material was purified by preparative HPLC to yield the title compound as a white solid. MS (m/e): 271.4 ([M−H]−, 100%).

WORKUP

后处理

  1. customThe crude material was purified by preparative HPLC