HuagongsheHuagongshe Chemistry Print Report · For research reference only
(+-)-2-Butanol → 2-Sec-butoxy-5-methanesulfonyl-benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (+-)-2-Butanol | HCID 6568 | — |
| Reactant | 2-Chloro-5-(methylsulphonyl)benzoic acid | HCID 2329132 | — |
| Product | 2-Sec-butoxy-5-methanesulfonyl-benzoic acid | HCID 21100258 | — |
Reaction Steps
Prepared in analogy to Example A1 (b) from 2-chloro-5-methanesulfonyl-benzoic acid (Example A1(a)) and rac-butan-2-ol. The crude material was purified by preparative HPLC to yield the title compound as a white solid. MS (m/e): 271.4 ([M−H]−, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07220744B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-6ec63ae73e8945939112276519955628 |
| Source note | uspto-grants-2007_05 |