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HRID1352324

反应详情

EQUATION

反应方程式

HRID 1352324 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CCCCS(=O)(=O)c1cnc(N2CCN(C(=O)OC(C)(C)C)CC2)s1
HCID68406275

未命名化合物

PRODUCTS

生成物

1
结构：CCCCS(=O)(=O)c1cnc(N2CCNCC2)s1.Cl
HCID21100183

未命名化合物

收率 92%

PROCEDURE

实验过程

Prepared in analogy to example 4 (d) from 4-[5-(butane-1-sulfonyl)-thiazol-2-yl]-piperazine-1-carboxylic acid tert-butyl ester and hydrogen chloride solution. The crude material was purified by recrystallisation from ether to afford the title compound as an off-white crystalline solid (yield 92%). MS (m/e): 290.0 (M+H+, 100%).

WORKUP

后处理

  1. customThe crude material was purified by recrystallisation from ether