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HRID1352363

反应详情

EQUATION

反应方程式

HRID 1352363 的结构方程式

REACTANTS

反应物

2
结构：FC(F)(F)c1nnc(N2CCNCC2)s1.O=C(O)C(F)(F)F
HCID21100199

未命名化合物

结构：CS(=O)(=O)c1ccc(OCC2CC2)c(C(=O)O)c1
HCID21100228

2-(Cyclopropylmethoxy)-5-(methylsulfonyl)benzoic acid

C12H14O5S

PRODUCTS

生成物

1
结构：CS(=O)(=O)c1ccc(OCC2CC2)c(C(=O)N2CCN(c3nnc(C(F)(F)F)s3)CC2)c1
HCID11612866

未命名化合物

PROCEDURE

实验过程

Prepared in analogy to example 1 (b) from 2-cyclopropylmethoxy-5-methanesulfonyl-benzoic acid (Example A5) and 1-(5-trifluoromethyl-[1,3,4]thiadiazol-2-yl)-piperazine trifluoroacetate (Example 62(b)). The crude material was purified by chromatography (SiO2, dichloromethane/methanol 98:2) to yield the title compound as a colorless solid. MS (m/e): 491.2 (M+H+, 100%).

WORKUP

后处理

  1. customThe crude material was purified by chromatography (SiO2, dichloromethane/methanol 98:2)