HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13524712, compound → HCID 20654283, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13524712 | HCID 13524712 | — |
| Reactant | HCID 20654282 | HCID 20654282 | — |
| Product | HCID 20654283 | HCID 20654283 | — |
Reaction Steps
The title compound was prepared according to the oxalyl chloride/DMSO oxidation step of Example 46 starting with (4-fluoro)phenyl-[(7RS,9aSR)-2-(pyrimidin-2-yl)-2,3,4,6,7,8,9,9a-octahydro-1H-pyrido[1,2-a]pyrazin-7-yl]-methanol (Example 46). 13C NMR (CDCl3): δ 27.3, 28.3, 48.6, 54.1, 56.7, 59.9, 110.1, 115.77, 116.05, 131.20, 131.32, 132.4, 158.0, 161.1, 163.4, 166.7. HRMS calcd for C19H21FN4O: 340.1699, found: 340.1539.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07220753B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-0da022006e7c488d9573bd7c847b0036 |
| Source note | uspto-grants-2007_05 |