HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorophenyl isocyanate → HCID 21101813, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorophenyl isocyanate | HCID 70955 | — |
| Reactant | HCID 21101968 | HCID 21101968 | — |
| Reactant | Ethyl acetate hexane | HCID 21226206 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21101813 | HCID 21101813 | — |
Reaction Steps
7-Fluoro-4-(piperazin-1-yl)quinoline (0.29 g, 1.25 mmol) and 4-fluorophenyl isocyanate (142 μL, 1.25 mmol) in THF (10 mL) are reacted according to method C yielding the product as colorless crystals after column chromatography with hexane-EtOAc.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07220856B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-9e2f4ebac1e44e49a13098131b39aaf3 |
| Source note | uspto-grants-2007_05 |