HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → HCID 21101702, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 21101706 | HCID 21101706 | — |
| Product | HCID 21101702 | HCID 21101702 | — |
Reaction Steps
4-[4-(tert-Butoxycarbonyl)piperazin-1-yl]-7-chloroquinol-2-one (150 mg, 0.4 mmol), sodium hydride (15 mg, 0.6 mmol), N-phenyl(trifluoromethylsulfon)imide (208 mg, 0.56 mmol), and ethanolamine (100 μL, 1.65 mmol) are treated according to method E yielding the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07220856B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-72999e9a4898489693912e373a81e3d3 |
| Source note | uspto-grants-2007_05 |