HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorophenyl isocyanate → HCID 21101772, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorophenyl isocyanate | HCID 70955 | — |
| Reactant | HCID 21101961 | HCID 21101961 | — |
| Reactant | Ethyl acetate hexane | HCID 21226206 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21101772 | HCID 21101772 | — |
Reaction Steps
7-Chloro-4-(3-methylpiperazin-1-yl)quinoline (0.13 g, 0.5 mmol) and 4-fluorophenyl isocyanate (57 μL, 0.5 mmol) in CH2Cl2 (10 mL) are reacted according to method C yielding the title product after column chromatography with hexane-EtOAc.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07220856B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-4e0791e4226c4f1fac0c357e1bdce9ad |
| Source note | uspto-grants-2007_05 |