HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,7-Dichloroquinoline → HCID 21101960, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,7-Dichloroquinoline | HCID 6866 | — |
| Reactant | 2,6-Dimethylpiperazine | HCID 66056 | — |
| Reactant | Dichloromethane methanol | HCID 21226129 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 21101960 | HCID 21101960 | — |
Reaction Steps
4,7-Dichloroquinoline (0.40 g, 2.0 mmol) and. 2,6-dimethylpiperazine (0.57 g, 5.0 mmol) in n-butanol (20 mL) are reacted according to method B yielding the title product after column chromatography with CH2Cl2-MeOH.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07220856B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-e16e78110e504fe1a9844fa3c2d3d599 |
| Source note | uspto-grants-2007_05 |