HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Isocyanato-4-methoxybenzene → HCID 21101795, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Isocyanato-4-methoxybenzene | HCID 79443 | — |
| Reactant | 7-Chloro-4-(piperazin-1-yl)quinoline | HCID 738389 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21101795 | HCID 21101795 | — |
Reaction Steps
7-Chloro-4-(piperazin-1-yl)quinoline (316 mg, 1.28 mmol) and 4-methoxyphenyl isocyanate (194 μL, 1.50 mmol) in THF (10 mL) are reacted according to method C yielding the title product as a colorless needles after column chromatography with hexane-EtOAc and recrystallization from ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07220856B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-c98317d5818548cba05daa94655b72a2 |
| Source note | uspto-grants-2007_05 |