HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-Chloro-4-(piperazin-1-yl)quinoline → HCID 21101697, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-Chloro-4-(piperazin-1-yl)quinoline | HCID 738389 | — |
| Reactant | 1-Isocyanatoadamantane | HCID 2059995 | — |
| Reactant | Ethyl acetate hexane | HCID 21226206 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21101697 | HCID 21101697 | — |
Reaction Steps
7-Chloro-4-(piperazin-1-yl)quinoline (124 mg, 0.5 mmol) and 1-adamantyl isocyanate (89 mg, 0.5 mmol) in CH2Cl2 (5 mL) are reacted according to method C yielding the title product as a colorless solid after column chromatography with hexane-EtOAc.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07220856B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-1fc78abc1f354b0d82b165bb70b355f7 |
| Source note | uspto-grants-2007_05 |