HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diphenyl N-Cyanocarbonimidate → HCID 87869961, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diphenyl N-Cyanocarbonimidate | HCID 688090 | — |
| Reactant | 7-Chloro-4-(piperazin-1-yl)quinoline | HCID 738389 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 87869961 | HCID 87869961 | — |
Reaction Steps
7-Chloro-4-(piperazin-1-yl)quinoline (798 mg, 3.22 mmol) and diphenyl cyanocarbonimidate (853 mg, 3.58 mmol) in THF (10 mL) are stirred at room temp. for 15 h. The reaction mixture is diluted with ether, and the precipitate is filtered off to yield the title product as a colorless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07220856B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-039fa00f4bc947349a3166e837a21117 |
| Source note | uspto-grants-2007_05 |