HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium tert-butoxide → HCID 87870131, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Reactant | HCID 87869961 | HCID 87869961 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 87870131 | HCID 87870131 | — |
Reaction Steps
7-Chloro-4-[4-(cyanimino(phenoxy)methyl)piperazin-1-yl]quinoline (196 mg, 0.5 mmol) and potassium tert-butoxide (62 mg, 0.55 mmol) in EtOH (5 mL) are stirred at room temp. for 4 h. The reaction mixture is concentrated, and the residue purified by column chromatography delivering the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07220856B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-b5ff85d316f94eb988f5d4a1f58271d4 |
| Source note | uspto-grants-2007_05 |