Diisopropylethylamine → HCID 21101724, compound

Participants

Role	Name	HCID	Charge
Reactant	Diisopropylethylamine	HCID 81531	—
Reactant	4-Nitrophenyl chloroformate	HCID 82129	—
Reactant	7-Chloro-4-(piperazin-1-yl)quinoline	HCID 738389	—
Reactant	HCID 20379954	HCID 20379954	—
Product	HCID 21101724	HCID 21101724	—

Reaction Steps

As described for example 78, 3-hydroxycycloheptyl-amine, p-nitrophenyl chloroformate, diisopropylethyl amine and 7-chloro-4-piperazinylquinoline are reacted to afford the product. LC-MS: 403 (M++1). 1H NMR (CDCl3) δ 8.75 (d, 1H), 8.05 (s, 1H), 7.96 (d, 1H), 7.45 (d, 1H), 6.84 (d, 1H), 4.50 (d, 1H), 4.10 (m, 2H), 3.65 (m, 4H), 3.20 (m, 4H), 2.38 (m, 1H), 2.0 (m, 3H), 1.80 (m, 4H), 1.40 (m, 2H).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07220856B2
Source dataset	uspto-grants-2007_05
ORD ID	ord-f816b9041c754cef82358d856a818454
Source note	uspto-grants-2007_05