HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 58864175, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | Propanoic acid, 2-isocyanato-, methyl ester (9CI) | HCID 2759403 | — |
| Reactant | 7-Chloro-4-(1-piperazinyl)-2-quinolinamine | HCID 21101748 | — |
| Product | HCID 58864175 | HCID 58864175 | — |
Reaction Steps
As described example 159, 7-chloro-4-(1-piperazinyl)-2-quinolinamine, 2-isocyanato-propanic acid-methyl ester, and diisopropylethyl amine, are reacted to give the product as a white solid. LC-MS: 392 (M++1). 1H NMR (DMSO-d6) δ 1.30 (d, 3H), 2.96 (br.s, 4H), 3.55 (m, 4H), 3.61 (s, 3H), 4.16 (m, 1H), 6.26 (s, 1H), 6.45 (br.s, 2H), 6.90 (d, 1H), 7.10 (dd, 1H), 7.38 (d, 1H), 7.75 (d, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07220856B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-c17df72999cf418e9893eea9d4512b52 |
| Source note | uspto-grants-2007_05 |