Diisopropylethylamine → HCID 72447322, compound

Participants

Reaction Steps

As described for 78, 2-methoxycarbonyl-cycloheptanone-oxime, 4-nitrophenyl chloroformate, diisopropyl(ethyl)amine, and 7-chloro-4-(1-piperazinyl)-2-quinolinamine are reacted to afford the product. LC-MS: 474 (M++1). 1H NMR (CDCl3) δ 7.75 (d, 1H), 7.60 (s, 1H), 7.18 (d, 1H), 6.15 (s, 1H), 4.80 (s, 2H), 3.80 (m, 5H), 3.75 (s, 3H), 3.15 (m, 4H), 2.90 (m, 1H), 2.40 (m, 1H), 2.05 (m, 2H), 1.72 (m, 2H), 1.60 (m, 3H), 1.45 (m, 1H).

Provenance & Evidence