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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1353461Generated: November 3, 2026

Diisopropylethylamine → HCID 58864160, compound

https://huagongshe.com/reaction/1353461

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiisopropylethylamineHCID 81531—
Reactant4-Nitrophenyl chloroformateHCID 82129—
ReactantMethyl 2-aminocycloheptane-1-carboxylateHCID 4650515—
Reactant7-Chloro-4-(1-piperazinyl)-2-quinolinamineHCID 21101748—
ProductHCID 58864160HCID 58864160—

Reaction Steps

As described for 78, 2-methoxycarbonyl cycloheptyl amine, 4-nitrophenyl chloroformate, diisopropyl(ethyl)amine, and 7-chloro-4-(1-piperazinyl)-2-quinolinamine are reacted to afford the product. LC-MS: 460 (M++1). 1H NMR (CDCl3) δ 7.72 (d, 1H), 7.60 (s, 1H), 7.18 (d, 1H), 6.15 (s, 1H), 5.50 (d, 1H), 4.70 (s, 2H), 4.15 (m, 1H), 3.70 (s, 3H), 3.60 (m, 4H), 3.10 (m, 4H), 2.95 (m, 1H), 2.00 (m, 1H), 1.85 (m, 3H), 1.65 (m, 5H), 1.45 (m, 1H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07220856B2
Source datasetuspto-grants-2007_05
ORD IDord-9f8368ea4a834c1c8a7a22ad3723cc01
Source noteuspto-grants-2007_05