HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cycloheptylamine → HCID 21101679, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cycloheptylamine | HCID 2899 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | 4-Nitrophenyl chloroformate | HCID 82129 | — |
| Reactant | 7-Chloro-4-(1-piperazinyl)-2-quinolinamine | HCID 21101748 | — |
| Product | HCID 21101679 | HCID 21101679 | — |
Reaction Steps
As described for example 78, cycloheptylamine, 4-nitrophenyl chloroformate, diisopropyl(ethyl)amine, and 7-chloro-4-(1-piperazinyl)-2-quinolinamine are reacted to afford the product as a light yellow solid. LC-MS: 402 (M++1). 1H NMR (CDCl3) δ 7.75 (d, 1H), 7.62 (s, 1H), 7.15 (d, 1H), 6.15 (s, 1H), 4.78 (s, 2H), 4.40 (d, 1H), 3.90 (m, 1H), 3.60 (m, 4H), 3.10 (m, 4H), 1.95 (m, 2H) 1.40–1.65 (m, 10H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07220856B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-ee413002eb6f4256baf432789e60159e |
| Source note | uspto-grants-2007_05 |