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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1353465Generated: November 1, 2026

Cycloheptylamine → HCID 21101679, compound

https://huagongshe.com/reaction/1353465

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCycloheptylamineHCID 2899—
ReactantDiisopropylethylamineHCID 81531—
Reactant4-Nitrophenyl chloroformateHCID 82129—
Reactant7-Chloro-4-(1-piperazinyl)-2-quinolinamineHCID 21101748—
ProductHCID 21101679HCID 21101679—

Reaction Steps

As described for example 78, cycloheptylamine, 4-nitrophenyl chloroformate, diisopropyl(ethyl)amine, and 7-chloro-4-(1-piperazinyl)-2-quinolinamine are reacted to afford the product as a light yellow solid. LC-MS: 402 (M++1). 1H NMR (CDCl3) δ 7.75 (d, 1H), 7.62 (s, 1H), 7.15 (d, 1H), 6.15 (s, 1H), 4.78 (s, 2H), 4.40 (d, 1H), 3.90 (m, 1H), 3.60 (m, 4H), 3.10 (m, 4H), 1.95 (m, 2H) 1.40–1.65 (m, 10H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07220856B2
Source datasetuspto-grants-2007_05
ORD IDord-ee413002eb6f4256baf432789e60159e
Source noteuspto-grants-2007_05