HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 21101676, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | 4-Nitrophenyl chloroformate | HCID 82129 | — |
| Reactant | 4-Fluoro-3-methoxyaniline | HCID 2774533 | — |
| Reactant | 7-Chloro-4-(1-piperazinyl)-2-quinolinamine | HCID 21101748 | — |
| Product | HCID 21101676 | HCID 21101676 | — |
Reaction Steps
As described for example 78, 4-fluoro-3-methoxy-aniline, 4-nitrophenyl chloroformate, diisopropyl(ethyl)amine, and 7-chloro-4-(1-piperazinyl)-2-quinolinamine are reacted to afford the product as a light yellow solid. LC-MS: 430 (M++1). 1H NMR (CD3OD) δ 8.25 (m, 2H), 7.82 (m, 1H), 7.45 (s, 1H), 7.40 (d, 2H), 7.20 (d, 1H), 6.40 (s, 1H), 3.95 (s, 3H), 3.80 (m, 4H), 3.25 (m, 4H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07220856B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-fb371bac2eb546f0be942817403b6ee8 |
| Source note | uspto-grants-2007_05 |