HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 21101664, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | 4-Nitrophenyl chloroformate | HCID 82129 | — |
| Reactant | 3-Amino-1-methylpyridin-2(1H)-one | HCID 15692208 | — |
| Reactant | 7-Chloro-4-(1-piperazinyl)-2-quinolinamine | HCID 21101748 | — |
| Product | HCID 21101664 | HCID 21101664 | — |
Reaction Steps
As described for example 78, 3-amino-1-methyl-2-pyridone, 4-nitrophenyl chloroformate, diisopropyl(ethyl)amine, and 7-chloro-4-(1-piperazinyl)-2-quinolinamine are reacted to afford the product. LC-MS: 413 (M++1). 1H NMR (CDCl3) δ 8.15 (dd, 1H), 8.02 (s, 1H), 7.74 (d, 1H), 7.65 (s, 1H), 7.20 (dd, 1H), 6.95 (dd, 1H), 6.25 (m, 1H), 6.16 (s, 1H), 5.00 (s, 2H), 3.80 (m, 4H), 3.62 (s, 3H), 3.20 (m, 4H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07220856B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-cbf4763715dc401ca0721816eb621c0b |
| Source note | uspto-grants-2007_05 |