HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 86591808, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | 4-Nitrophenyl chloroformate | HCID 82129 | — |
| Reactant | Methyl 2-aminocyclohexane-1-carboxylate | HCID 16639469 | — |
| Reactant | 7-Chloro-4-(1-piperazinyl)-2-quinolinamine | HCID 21101748 | — |
| Product | HCID 86591808 | HCID 86591808 | — |
Reaction Steps
As described for example 78, 2-amino-cyclohexanecarboxylic acid-methyl ester, 4-nitrophenyl chloroformate, diisopropyl(ethyl)amine, and 7-chloro-4-(1-piperazinyl)-2-quinolinamine are reacted to afford the product as a light yellow solid. LC-MS: 446 (M++1). 1H NMR (CD3OD) δ 1.20–1.40 (m, 4H), 1.90 (m, 3H), 2.10 (m, 1H), 2.45 (m, 1H), 3.30 (m, 4H), 3.70 (m, 8H), 6.35 (s, 1H), 7.38 (d, 1H), 7.60 (s, 1H), 790 (d, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07220856B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-62ca934868754588b351a51cac37d5a1 |
| Source note | uspto-grants-2007_05 |