Hydrochloric Acid → HCID 17984766, compound

HRID 1354033Notes

Reaction equation

HRID 1354033 reaction equation
Br[C:2]1[N:3]=[N:4][C:5]([C:8]2[CH:12]=[CH:11][S:10][CH:9]=2)=[CH:6][CH:7]=1.[ClH:13]>>[ClH:13].[Cl:13][C:2]1[N:3]=[N:4][C:5]([C:8]2[CH:12]=[CH:11][S:10][CH:9]=2)=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 17984761HCID 17984761, compound

Product 1

HCID 17984766HCID 17984766, compound

Procedure

A mixture of 3-bromo-6-thien-3-yl-pyridazine (1.39 g, 5.8 mmol) and conc. hydrochloric acid (25 ml) was stirred at reflux for 4.5 hours. The reaction mixture was evaporated and the product was isolated in quantitative yield (1.35 g, 5.8 mmol).

Workup

  1. temperatureat reflux for 4.5 hours
  2. customThe reaction mixture was evaporated
  3. customthe product was isolated in quantitative yield (1.35 g, 5.8 mmol)

Sources & evidence

ORD record
ord-c345800cf0cf48b88c4cd6f2b2416e30
Source dataset
uspto-grants-2007_05
Patent number
US07223753B2

Reaction notes

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