2-Morpholinoethylamine → HCID 21103270, compound
Reaction equation
C(O[C:4]([CH2:6][N:7]([S:15]([C:18]1[CH:23]=[CH:22][C:21]([O:24][CH3:25])=[CH:20][CH:19]=1)(=[O:17])=[O:16])[CH:8]([CH2:13]O)[C:9]([O:11][CH3:12])=[O:10])=[O:5])C.[NH2:26][CH2:27][CH2:28][N:29]1[CH2:34][CH2:33][O:32][CH2:31][CH2:30]1>>[CH3:25][O:24][C:21]1[CH:22]=[CH:23][C:18]([S:15]([N:7]2[CH2:6][C:4](=[O:5])[N:26]([CH2:27][CH2:28][N:29]3[CH2:34][CH2:33][O:32][CH2:31][CH2:30]3)[CH2:13][CH:8]2[C:9]([O:11][CH3:12])=[O:10])(=[O:17])=[O:16])=[CH:19][CH:20]=1Participants
3
Procedure
A title compound was prepared by the same method as in Example 4, except that the compound of Example 3 and N-(2-aminoethyl)morpholine were used to prepare a yellow oil (yield 74%).
Sources & evidence
- ORD record
- ord-2bd6e156efc84aa5a515d45a2e76f1fa
- Source dataset
- uspto-grants-2007_05
- Patent number
- US07223751B2
Reaction notes
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