Methylamine → HCID 21103271, compound

HRID 1354081Notes

Reaction equation

HRID 1354081 reaction equation
C([O:3][C:4]([CH2:6][N:7]([S:15]([C:18]1[CH:23]=[CH:22][C:21]([O:24][CH3:25])=[CH:20][CH:19]=1)(=[O:17])=[O:16])[CH:8]([CH2:13]O)[C:9]([O:11][CH3:12])=[O:10])=O)C.[CH3:26][NH2:27]>>[CH3:25][O:24][C:21]1[CH:22]=[CH:23][C:18]([S:15]([N:7]2[CH2:6][C:4](=[O:3])[N:27]([CH3:26])[CH2:13][CH:8]2[C:9]([O:11][CH3:12])=[O:10])(=[O:17])=[O:16])=[CH:19][CH:20]=1

Participants

3

Reactant 2

HCID 6329MethylamineHCID 11234214HCID 11234214, compound

Product 1

HCID 21103271HCID 21103271, compound

Procedure

A title compound was prepared by the same method as in Example 4, except that it was prepared from the compound of Example 3 and methylamine, and recrystallized with ethylacetate/hexane to obtain a white solid (yield 73%)

Workup

  1. customrecrystallized with ethylacetate/hexane

Sources & evidence

ORD record
ord-b73cce3f587748289e12213b293ee0ed
Source dataset
uspto-grants-2007_05
Patent number
US07223751B2

Reaction notes

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