HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12619394, compound → HCID 250480, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12619394 | HCID 12619394 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 250480 | HCID 250480 | 93% |
Reaction Steps
2-Allyl-2-propylcyclohexanone (2.96 g, 16.4 mmol) and PtO2 (300 mg) were combined in MeOH (100 mL) and hydrogenated at 1 atm for 4 hrs. The catalyst was filtered off and the solvent evaporated to afford 2.78 g (93%) of 2,2-dipropylcyclohexanone as a colorless liquid. MS (CI) 183 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07223767B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-dc6c93822f5e46189e994fdab7191fa3 |
| Source note | uspto-grants-2007_05 |