HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetoxyacetyl chloride → HCID 21104418, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetoxyacetyl chloride | HCID 26297 | — |
| Reactant | HCID 9845828 | HCID 9845828 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Solvent | Diisopropylethylamine | HCID 81531 | — |
| Product | HCID 21104418 | HCID 21104418 | — |
Reaction Steps
By using 4-[2-(3-fluoro-phenyl)-6-trifluoromethyl-pyrazolo[1,5-a]pyridin-3-yl]benzenesulfonamide (0.15 g 0.35 mmol), diisopropylethylamine (Aldrich) (150 μl ), 4-dimethylaminopyridine (0.04 g 0.32 mmol) and acetoxyacetyl chloride (Aldrich) (0.109 g 0.8 mmol), the title compound was obtained in the manner of Example 19 as a white solid (0.14 g 75%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07223772B1 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-3eafc36aa09441ad833a0c60e782a578 |
| Source note | uspto-grants-2007_05 |