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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1354276Generated: November 2, 2026

Methanol → HCID 21104871, compound

https://huagongshe.com/reaction/1354276

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantHCID 58866161HCID 58866161—
CatalystPalladiumHCID 23938—
ProductHCID 21104871HCID 21104871—

Reaction Steps

The above compound (6) (316 mg) was dissolved in methanol (25 mL) and 10% Pd—C (40 mg) was added, and then the mixture was stirred under a hydrogen atmosphere at room temperature for 2 hours. The catalyst was removed by filtration and the filtrate was concentrated under reduced pressure to obtain the titled compound (242 mg) as a colorless powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07223779B2
Source datasetuspto-grants-2007_05
ORD IDord-86afaaa1fa474c74bd5160efd5fe7704
Source noteuspto-grants-2007_05