HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 21104871, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 58866161 | HCID 58866161 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 21104871 | HCID 21104871 | — |
Reaction Steps
The above compound (6) (316 mg) was dissolved in methanol (25 mL) and 10% Pd—C (40 mg) was added, and then the mixture was stirred under a hydrogen atmosphere at room temperature for 2 hours. The catalyst was removed by filtration and the filtrate was concentrated under reduced pressure to obtain the titled compound (242 mg) as a colorless powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07223779B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-86afaaa1fa474c74bd5160efd5fe7704 |
| Source note | uspto-grants-2007_05 |