HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 69520324, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86598975 | HCID 86598975 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 69520324 | HCID 69520324 | — |
Reaction Steps
The product from step (c) (45 mg) was dissolved in 4M HCl in dioxane (5 ml). The resulting solution was stirred at room temperature for 15 minutes, then the solvent was evaporated off. The residue was recrystallised from diethyl ether/ethanol to give the title compound as a white solid (19 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07223794B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-101fdc1c64be4175a6927b9a5eabfeda |
| Source note | uspto-grants-2007_05 |