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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1354673Generated: October 31, 2026

Aniline → HCID 21105308, compound

https://huagongshe.com/reaction/1354673

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAnilineHCID 6115—
Reactant(4-Aminophenoxy)benzeneHCID 8764—
Reactantp-FluoronitrobenzeneHCID 9590—
Reactant1,1'-CarbonyldiimidazoleHCID 68263—
Reactant3-(Dimethylamino)pyrrolidineHCID 2758519—
ReactantHCID 178418361HCID 178418361—
ProductHCID 21105308HCID 21105308—

Reaction Steps

Dimethylpyrrolidin-3-ylamine was reacted with 4-fluoronitrobenzene, the resulting nitro compound was reduced with hydrogen and finally the aniline was reacted with CDI and 4-phenoxyaniline by method A, B and C. This resulted in the product with the molecular weight of 416.53 (C25H28N4O2); MS (ESI): 417 (M+H+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07223788B2
Source datasetuspto-grants-2007_05
ORD IDord-62f27a6510f44d81985c0d2b3b57c4a4
Source noteuspto-grants-2007_05