HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → HCID 18507677, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | Carbonic acid-guanidine (1:1) | HCID 286947 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | 3-Oxo-3-(3,4,5-trimethoxyphenyl)propanenitrile | HCID 18507691 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18507677 | HCID 18507677 | — |
Reaction Steps
From 3,4,5-trimethoxybenzoylacetonitrile and N,N-dimethylformamide dimethyl acetal. Then treatment with guanidine carbonate and sodium methylate in methanol. EI-MS m/e (%): 286 (M+, 100), 271 ([M—CH3]+, 44), 243 (27), 228 (15), 213 (30), 157 (16).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586441B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-3d513dd741d64d789929f29c35cad1b0 |
| Source note | uspto-grants-2003_07 |