HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 18507567, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Iodophenylacetic acid | HCID 2780090 | — |
| Reactant | HCID 18507677 | HCID 18507677 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18507567 | HCID 18507567 | — |
Reaction Steps
From 2-iodophenylacetic acid, thionyl chloride and N,N-in dichloromethane. Then treatment with 2-amino-5-cyano-4-(3,4,5-trimethoxyphenyl)pyrimidine and pyridine in dichloromethane. ES-MS m/e (%): 553 (M+Na+, 15), 531 (M+H+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586441B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-89e5041e619a4241967d318fd0ff14dd |
| Source note | uspto-grants-2003_07 |