HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → HCID 18507581, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | Carbonic acid-guanidine (1:1) | HCID 286947 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | 3-(2H-1,3-Benzodioxol-5-yl)-3-oxopropanenitrile | HCID 19616538 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18507581 | HCID 18507581 | — |
Reaction Steps
From 3-benzo[1,3]dioxol-5-yl-3-oxo-propionitrile and N,N-dimethylformamide dimethyl acetal. Then treatment with guanidine carbonate and sodium methylate in methanol. EI-MS m/e (%): 240 (M+, 100), 239 ([M—H]+, 62).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586441B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-ff3f02e6c8bf4f49b5d8de253a91c6ef |
| Source note | uspto-grants-2003_07 |