HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 1120784, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 3,4,5-Trimethoxybenzaldehyde | HCID 6858 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 2-Cyanoethanethioamide | HCID 1416277 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | 2-Hydroxybutanedinitrile | HCID 21253562 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 1120784 | HCID 1120784 | — |
Reaction Steps
From 3,4,5-trimethoxybenzaldehyde, malonitrile, cyanothioacetamide and piperidine in EtOH. Then treatment with methyl iodide and sodium methylate in methanol. EI-MS m/e (%): 356 (M+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586441B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-07405e3db91541cba95f28719a09f5ac |
| Source note | uspto-grants-2003_07 |