HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl bromide → 2-Amino-4-butylsulfanyl-6-phenyl-pyrimidine-5-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl bromide | HCID 8002 | — |
| Reactant | Sodium ethoxide | HCID 2723922 | — |
| Reactant | HCID 178509378 | HCID 178509378 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-Amino-4-butylsulfanyl-6-phenyl-pyrimidine-5-carbonitrile | HCID 18507672 | — |
Reaction Steps
From 2-amino-4-phenyl-6-thioxo-1,6-dihydro-pyrimidine-5-carbonitrile, butyl bromide and sodium ethylate in ethanol. EI-MS m/e (%): 284 (M+, 48), 283 ([M—H]+, 100), 241 (([M—C3H7]+, 95), 228 (([M—C2H5CH═CH2]+, 92).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586441B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-838201fbb8d44b8b8ccfd24ca6fa4b4d |
| Source note | uspto-grants-2003_07 |