2-Methoxyethylamine → HCID 18507660, compound

HRID 1355751Notes

Reaction equation

HRID 1355751 reaction equation
[NH2:1][C:2]1[N:7]=[C:6]([C:8]2[O:9][CH:10]=[CH:11][CH:12]=2)[C:5]([C:13]#[N:14])=[C:4](S(C)(=O)=O)[N:3]=1.[CH3:19][O:20][CH2:21][CH2:22][NH2:23]>COCCOC>[NH2:1][C:2]1[N:7]=[C:6]([C:8]2[O:9][CH:10]=[CH:11][CH:12]=2)[C:5]([C:13]#[N:14])=[C:4]([NH:23][CH2:22][CH2:21][O:20][CH3:19])[N:3]=1

Participants

4

Reactant 2

HCID 80182-MethoxyethylamineHCID 185073992-Amino-4-furan-2-yl-6-methanesulfonyl-pyrimidine-5-carbonitrile

Product 1

HCID 18507660HCID 18507660, compound

Reagents, catalysts & solvents 1

HCID 80711,2-DimethoxyethaneSolvent

Procedure

From 2-amino-4-furan-2-yl-6-methanesulfonyl-pyrimidine-5-carbonitrile and 2-methoxyethylamine in DME. EI-MS m/e (%): 259 (M+, 15), 214 ([M—MeOCH2]+, 100), 201 ([M—MeOCH═CH2]+, 78).

Sources & evidence

ORD record
ord-5b7bc810d0674a10bbcbc46dedc82d8b
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

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