Piperidine → HCID 18507502, compound

HRID 1355764Notes

Reaction equation

HRID 1355764 reaction equation
[NH2:1][C:2]1[N:7]=[C:6](S(C)(=O)=O)[C:5]([C:12]#[N:13])=[C:4]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[N:3]=1.[NH:20]1[CH2:25][CH2:24][CH2:23][CH2:22][CH2:21]1>COCCOC>[NH2:1][C:2]1[N:3]=[C:4]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[C:5]([C:12]#[N:13])=[C:6]([N:20]2[CH2:25][CH2:24][CH2:23][CH2:22][CH2:21]2)[N:7]=1

Participants

4

Reactant 2

HCID 8082PiperidineHCID 18507408HCID 18507408, compound

Product 1

HCID 18507502HCID 18507502, compound

Reagents, catalysts & solvents 1

HCID 80711,2-DimethoxyethaneSolvent

Procedure

From 2-amino-4-methanesulfonyl-6-phenyl-pyrimidine-5-carbonitrile and piperidine in DME. EI-MS m/e (%): 279 (M+, 32), 278 ([M—H]+, 100).

Sources & evidence

ORD record
ord-d11d079849884abdb6b848ff267bd4b3
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

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