HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Phenylethanol → HCID 9901475, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Phenylethanol | HCID 6054 | — |
| Reactant | Styrene | HCID 7501 | — |
| Reactant | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Reactant | HCID 18507370 | HCID 18507370 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 9901475 | HCID 9901475 | — |
Reaction Steps
From 2-amino-4-chloro-6-phenyl-pyrimidine-5-carbonitrile, 2-phenylethanol and DBU in DME. EI-MS m/e (%): 316 (M+, 4), 212 ([M—PhCH═CH2]+, 100), 184 (28), 170 (20), 104 ([PhCH═CH2]+, 84), 77 (20).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586441B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-c543d6f308ee49a1a6a688899582c9e1 |
| Source note | uspto-grants-2003_07 |