Ethanol → HCID 18507208, compound

HRID 1355789Notes

Reaction equation

HRID 1355789 reaction equation
[NH2:1][C:2]1[N:7]=[C:6]([C:8]2[CH:16]=[CH:15][C:11]3[O:12][CH2:13][O:14][C:10]=3[CH:9]=2)[C:5]([C:17]#[N:18])=[C:4](S(C)(=O)=O)[N:3]=1.C1CCN2C(=NCCC2)CC1.[CH2:34]([OH:36])[CH3:35]>>[NH2:1][C:2]1[N:7]=[C:6]([C:8]2[CH:16]=[CH:15][C:11]3[O:12][CH2:13][O:14][C:10]=3[CH:9]=2)[C:5]([C:17]#[N:18])=[C:4]([O:36][CH2:34][CH3:35])[N:3]=1

Participants

4

Reactant 3

HCID 702EthanolHCID 811841,8-Diazabicyclo(5.4.0)undec-7-eneHCID 18507322HCID 18507322, compound

Product 1

HCID 18507208HCID 18507208, compound

Procedure

From 2-amino-4-benzo[1,3]dioxol-5-yl-6-methanesulfonyl-pyrimidine-5-carbonitrile, ethanol and DBU in DMB. EI-MS rn/e 2%) 284 (M+, 100), 214 (32).

Sources & evidence

ORD record
ord-329d0df32e9b4f278f2e118642f59896
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

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