Propylamine → HCID 18507630, compound

HRID 1355792Notes

Reaction equation

HRID 1355792 reaction equation
[NH2:1][C:2]1[N:7]=[C:6](S(C)(=O)=O)[C:5]([C:12]#[N:13])=[C:4]([C:14]2[CH:19]=[C:18]([O:20][CH3:21])[C:17]([O:22][CH3:23])=[C:16]([O:24][CH3:25])[CH:15]=2)[N:3]=1.[CH2:26]([NH2:29])[CH2:27][CH3:28]>COCCOC>[NH2:1][C:2]1[N:7]=[C:6]([NH:29][CH2:26][CH2:27][CH3:28])[C:5]([C:12]#[N:13])=[C:4]([C:14]2[CH:19]=[C:18]([O:20][CH3:21])[C:17]([O:22][CH3:23])=[C:16]([O:24][CH3:25])[CH:15]=2)[N:3]=1

Participants

4

Reactant 2

HCID 7852PropylamineHCID 18507557HCID 18507557, compound

Product 1

HCID 18507630HCID 18507630, compound

Reagents, catalysts & solvents 1

HCID 80711,2-DimethoxyethaneSolvent

Procedure

From 2-amino-4-methanesulfonyl-6-(3,4,5-trimethoxy-phenyl)-pyrimidine-5-carbonitrile and propylamine in DME. ES-MS m/e (%): 382 (M+K+, 10), 366 (M+Na+, 20), 344 (M+H+, 100).

Sources & evidence

ORD record
ord-663976e29323439c9b5c23ad297022af
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

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