Ethanethiol → HCID 18507393, compound

HRID 1355795Notes

Reaction equation

HRID 1355795 reaction equation
[NH2:1][C:2]1[N:7]=[C:6]([C:8]2[CH:16]=[CH:15][C:11]3[O:12][CH2:13][O:14][C:10]=3[CH:9]=2)[C:5]([C:17]#[N:18])=[C:4]([S:19]([CH3:22])(=O)=O)[N:3]=1.[CH2:23](S)C.C1CCN2C(=NCCC2)CC1>COCCOC>[NH2:1][C:2]1[N:7]=[C:6]([C:8]2[CH:16]=[CH:15][C:11]3[O:12][CH2:13][O:14][C:10]=3[CH:9]=2)[C:5]([C:17]#[N:18])=[C:4]([S:19][CH2:22][CH3:23])[N:3]=1

Participants

5

Reactant 3

HCID 6343EthanethiolHCID 811841,8-Diazabicyclo(5.4.0)undec-7-eneHCID 18507322HCID 18507322, compound

Product 1

HCID 18507393HCID 18507393, compound

Reagents, catalysts & solvents 1

HCID 80711,2-DimethoxyethaneSolvent

Procedure

From 2-amino-4-benzo[1,3]dioxol-5-yl-6-methanesulfonyl-pyrimidine-5-carbonitrile, ethyl mercaptan and DBU in DME. EI-MS m/e (%): 300 (M+, 74), 299 ([M—H]+, I100).

Sources & evidence

ORD record
ord-9b237c58d838408283a382531cf6c40b
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

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