2-Propanol, sodium salt (1:1) → HCID 18507466, compound

HRID 1355801Notes

Reaction equation

HRID 1355801 reaction equation
[NH2:1][C:2]1[N:7]=[C:6]([C:8]2[CH:16]=[CH:15][C:11]3[O:12][CH2:13][O:14][C:10]=3[CH:9]=2)[C:5]([C:17]#[N:18])=[C:4](S(C)(=O)=O)[N:3]=1.[CH3:23][CH:24]([CH3:26])[O-:25].[Na+]>C(O)(C)C>[NH2:1][C:2]1[N:7]=[C:6]([C:8]2[CH:16]=[CH:15][C:11]3[O:12][CH2:13][O:14][C:10]=3[CH:9]=2)[C:5]([C:17]#[N:18])=[C:4]([O:25][CH:24]([CH3:26])[CH3:23])[N:3]=1

Participants

4

Reactant 2

HCID 109204432-Propanol, sodium salt (1:1)HCID 18507322HCID 18507322, compound

Product 1

HCID 18507466HCID 18507466, compound

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

From 2-amino-4-benzo[1,3]dioxol-5-yl-6-methanesulfonyl-pyrimidine-5-carbonitrile and sodium isopropoxide in isopropanol. ES-MS m/e (%): 299 (M+H+, 100).

Sources & evidence

ORD record
ord-edf738c468d54d769d4a40888e8f81de
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

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