HCID 9921990, compound → HCID 18507345, compound

HRID 1355833Notes

Reaction equation

HRID 1355833 reaction equation
[NH2:1][C:2]1[N:7]=[C:6]([C:8]2[O:9][CH:10]=[CH:11][CH:12]=2)[C:5]([C:13]#[N:14])=[C:4](/[CH:15]=[CH:16]/[C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[N:3]=1.[H][H]>[Pd].C1COCC1>[NH2:1][C:2]1[N:7]=[C:6]([C:8]2[O:9][CH:10]=[CH:11][CH:12]=2)[C:5]([C:13]#[N:14])=[C:4]([CH2:15][CH2:16][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[N:3]=1

Participants

5

Reactant 2

HCID 9921990HCID 9921990, compoundHCID 178418361HCID 178418361, compound

Product 1

HCID 18507345HCID 18507345, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 8028TetrahydrofuranSolvent

Procedure

From (E)-2-Amino-4-furan-2-yl-6-styryl-pyrimidine-5-carbonitrile, hydrogen and palladium on charcoal in THF. ES-MS m/e (%): 291 (M+H+, 100).

Sources & evidence

ORD record
ord-f65ec91a09f545a39566db571fdabee7
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

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