HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Acrylate → HCID 70003621, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | HCID 18507226 | HCID 18507226 | — |
| Catalyst | HCID 178418476 | HCID 178418476 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 70003621 | HCID 70003621 | — |
Reaction Steps
From 4-furan-2-yl-5-iodo-pyrimidin-2-ylamine, methyl acrylate, bis(triphenylphosphine)palladium(II) chloride and cesium carbonate in dioxane. EI-MS m/e (%): 245 (M+, 54), 228 ([M—NH3]+, 100), 186 ([M—CO2Me]+, 56), 158 (52).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586441B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-42c772149e4d415c8b1e41a90ad1884d |
| Source note | uspto-grants-2003_07 |