HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylonitrile → HCID 18507315, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylonitrile | HCID 7855 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | 4-Furan-2-yl-5-iodo-6-methylsulfanyl-pyrimidin-2-ylamine | HCID 18507589 | — |
| Catalyst | HCID 178418476 | HCID 178418476 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 18507315 | HCID 18507315 | — |
Reaction Steps
From 4-furan-2-yl-5-iodo-6-methylsulfanyl-pyrimidin-2-ylamine, acrylonitrile, bis(triphenylphosphine)palladium(II) chloride and cesium carbonate in dioxane. EI-MS m/e (%): 258 (M+, 76), 241 ([M—NH3]+, 100), 150 (56), 114 (32).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586441B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-58547058a24641a9ab3493e7834c2489 |
| Source note | uspto-grants-2003_07 |