2-Morpholinoethylamine → HCID 18507495, compound

HRID 1355856Notes

Reaction equation

HRID 1355856 reaction equation
[Br:1][C:2]1[C:3]([C:12]2[O:13][CH:14]=[CH:15][CH:16]=2)=[N:4][C:5]([NH2:11])=[N:6][C:7]=1S(C)=O.[NH2:17][CH2:18][CH2:19][N:20]1[CH2:25][CH2:24][O:23][CH2:22][CH2:21]1>O1CCOCC1>[Br:1][C:2]1[C:7]([NH:17][CH2:18][CH2:19][N:20]2[CH2:25][CH2:24][O:23][CH2:22][CH2:21]2)=[N:6][C:5]([NH2:11])=[N:4][C:3]=1[C:12]1[O:13][CH:14]=[CH:15][CH:16]=1

Participants

4

Reactant 2

HCID 4082852-MorpholinoethylamineHCID 185072865-Bromo-4-furan-2-yl-6-methanesulfinyl-pyrimidin-2-ylamine

Product 1

HCID 18507495HCID 18507495, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

From 5-bromo-4-furan-2-yl-6-methanesulfinyl-pyrimidin-2-yl-amine and 4-(2-aminoethyl)morpholine in dioxane. ES-MS m/e (%): 370 (M{81Br}+H+, 100), 368 (M{79Br}+H+, 97).

Sources & evidence

ORD record
ord-6403860e50cd4a399dfd27b8ad5b4488
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

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