2-Methoxyethylamine → HCID 18507618, compound

HRID 1355874Notes

Reaction equation

HRID 1355874 reaction equation
[Cl:1][C:2]1[C:3]([C:12]2[O:13][CH:14]=[CH:15][CH:16]=2)=[N:4][C:5]([NH2:11])=[N:6][C:7]=1S(C)=O.[CH3:17][O:18][CH2:19][CH2:20][NH2:21]>COCCOC>[Cl:1][C:2]1[C:7]([NH:21][CH2:20][CH2:19][O:18][CH3:17])=[N:6][C:5]([NH2:11])=[N:4][C:3]=1[C:12]1[O:13][CH:14]=[CH:15][CH:16]=1

Participants

4

Reactant 2

HCID 80182-MethoxyethylamineHCID 18507343HCID 18507343, compound

Product 1

HCID 18507618HCID 18507618, compound

Reagents, catalysts & solvents 1

HCID 80711,2-DimethoxyethaneSolvent

Procedure

From 5-chloro-4-furan-2-yl-6-methanesulfinyl-pyrimidin-2-yl-amine and 2-methoxyethylamine in DME. ES-MS m/e (%): 271 (M{37Cl}+H+, 43), 269 (M{35Cl}+H+, 100).

Sources & evidence

ORD record
ord-c68067ba98444dabb96838ed4548a1ec
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

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