2-(Dimethylamino)ethanol → HCID 18507559, compound

HRID 1355875Notes

Reaction equation

HRID 1355875 reaction equation
[NH2:1][C:2]1[N:7]=[C:6]([O:8]S(C(F)(F)F)(=O)=O)[C:5]([N+:16]([O-:18])=[O:17])=[C:4]([C:19]2[O:20][CH:21]=[CH:22][CH:23]=2)[N:3]=1.[CH3:24][N:25]([CH3:29])[CH2:26][CH2:27]O.C1CCN2C(=NCCC2)CC1>COCCOC>[CH3:24][N:25]([CH3:29])[CH2:26][CH2:27][O:8][C:6]1[C:5]([N+:16]([O-:18])=[O:17])=[C:4]([C:19]2[O:20][CH:21]=[CH:22][CH:23]=2)[N:3]=[C:2]([NH2:1])[N:7]=1

Participants

5

Reactant 3

HCID 79022-(Dimethylamino)ethanolHCID 811841,8-Diazabicyclo(5.4.0)undec-7-eneHCID 86583748Trifluoromethanesulfonic acid 2-amino-6-furan-2-yl-5-nitro-pyrimidin-4-yl ester

Product 1

HCID 18507559HCID 18507559, compound

Reagents, catalysts & solvents 1

HCID 80711,2-DimethoxyethaneSolvent

Procedure

From trifluoro-methanesulfonic acid 2-amino-6-furan-2-yl-5-nitro-pyrimidin-4-yl ester, 2-dimethylaminoethanol and DBU in DME. ES-MS m/e (%): 294 (M+H+, 100).

Sources & evidence

ORD record
ord-a050649d09864674bce70d4a6dec80a5
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

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